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B016662 - DRUG ANALYSIS III
Main information
Teaching Language
Course Content
Suggested readings
Learning Objectives
Prerequisites
Teaching Methods
Further information
Type of Assessment
Course program
Academic Year 2018-19
Coorte 2015 - 5-years Single Cycle Degree in PHARMACY
Course year
Fourth year - Second Semester
Belonging Department
Neurosciences, Psychology, Drug Research and Child Health (NEUROFARBA)
Course Type
Single education field course
Scientific Area
CHIM/08 - PHARMACEUTICAL CHEMISTRY
Credits
9
Teaching Hours
88
Teaching Term
04/03/2019 ⇒ 30/04/2020
Attendance required
No
Type of Evaluation
Final Grade
Course Content
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Course program
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Lectureship
- Last names A-L GUERRINI GABRIELLA
- Last names M-Z DEI SILVIA
- Last names M-Z VERGELLI CLAUDIA
Teaching Language - Last names A-L
italian language
Teaching Language - Last names M-Z
italian language
Course Content - Last names A-L
Identification of compounds registered in the FUI and in the EP.
Chemical and instrumental analysis of pharmaceutical structures and of some drug classes.
Chemical and instrumental analysis of pharmaceutical structures and of some drug classes.
Course Content - Last names M-Z
Identification of compounds registered in the FUI and in the EP.
Chemical and instrumental analysis of pharmaceutical structures and of some drug classes.
Chemical and instrumental analysis of pharmaceutical structures and of some drug classes.
Suggested readings - Last names A-L (Search our library's catalogue)
Slides are downloaded from Moodle (e-learning)
-Farmacopea Ufficiale italiana XII Ed.
-European Pharmacopoeia
-A. Carta, M. G. Mamolo , F. Novelli, S. Piras, Analisi Farmaceutica Qualitativa - EDISES
-F. Savelli, O. Bruno, Analisi Chimico Farmaceutica - Piccin
-Cavrini, Andrisano, Analisi farmaceutica. Metodi di riconoscimento e di separazione - Esculapio
-Farmacopea Ufficiale italiana XII Ed.
-European Pharmacopoeia
-A. Carta, M. G. Mamolo , F. Novelli, S. Piras, Analisi Farmaceutica Qualitativa - EDISES
-F. Savelli, O. Bruno, Analisi Chimico Farmaceutica - Piccin
-Cavrini, Andrisano, Analisi farmaceutica. Metodi di riconoscimento e di separazione - Esculapio
Suggested readings - Last names M-Z (Search our library's catalogue)
Slides are downloaded from Moodle (e-learning)
- Farmacopea Ufficiale italiana XII Ed.
- European Pharmacopoeia
- A. Carta, M. G. Mamolo , F. Novelli, S. Piras, Analisi Farmaceutica Qualitativa - EDISES
- F. Savelli, O. Bruno, Analisi Chimico Farmaceutica - Piccin
- Cavrini, Andrisano, Analisi farmaceutica. Metodi di riconoscimento e di separazione - Esculapio
- Farmacopea Ufficiale italiana XII Ed.
- European Pharmacopoeia
- A. Carta, M. G. Mamolo , F. Novelli, S. Piras, Analisi Farmaceutica Qualitativa - EDISES
- F. Savelli, O. Bruno, Analisi Chimico Farmaceutica - Piccin
- Cavrini, Andrisano, Analisi farmaceutica. Metodi di riconoscimento e di separazione - Esculapio
Learning Objectives - Last names A-L
The course consists of theoretical lectures (40 h) and practical individual exercitations (48h). The objective is to provide students with knowledge on the most useful chemical and instrumental methods for the identification and control of purity of substance of pharmaceutical interest according to FUI and EP.
Students will also learn methods for a systematic analysis of drugs.
Students will also learn methods for a systematic analysis of drugs.
Learning Objectives - Last names M-Z
The course consists of theoretical lectures (36 h) and practical individual exercitations (54h). The objective is to provide students with knowledge on the most useful chemical and instrumental methods for the identification and control of purity of substance of pharmaceutical interest according to FUI and EP.
Students will also learn methods for a systematic analysis of drugs.
Students will also learn methods for a systematic analysis of drugs.
Prerequisites - Last names A-L
Propaedeutic teachings are Drug Analysis I and II. Basic knowledge of Organic Chemistry is also required.
Prerequisites - Last names M-Z
Propaedeutic teachings are Drug Analysis I and II. Basic knowledge of Organic Chemistry is also required.
Teaching Methods - Last names A-L
Lectures supported by Power point presentation. Laboratory practice is carried out individually.
Didactic instruments: PC and video projector.
Didactic instruments: PC and video projector.
Teaching Methods - Last names M-Z
Lectures supported by Power point presentation. Laboratory practice is carried out individually.
Didactic instruments: PC and video projector.
Didactic instruments: PC and video projector.
Further information - Last names A-L
to make a date:
Dott. Guerrini: Tel 055 4573766, e-mail: gabriella.guerrini@unifi.it
Dott. Vergelli: Tel 055 4573790, e-mail: claudia.vergelli@unifi.it
Dipartimento di NEUROFARBA,
Sezione di Farmaceutica e Nutraceutica
Via U. Schiff, 6 - 50019 Sesto F.no - Firenze
Dott. Guerrini: Tel 055 4573766, e-mail: gabriella.guerrini@unifi.it
Dott. Vergelli: Tel 055 4573790, e-mail: claudia.vergelli@unifi.it
Dipartimento di NEUROFARBA,
Sezione di Farmaceutica e Nutraceutica
Via U. Schiff, 6 - 50019 Sesto F.no - Firenze
Further information - Last names M-Z
Dott. Vergelli: tel. 0554573790
e-mail claudia.vergelli@unifi.it
Dipartimento di NEUROFARBA
Sezione di Farmaceutica e Nutraceutica
Via U. Schiff, 6 - 50019 Sesto F.no - Firenze
e-mail claudia.vergelli@unifi.it
Dipartimento di NEUROFARBA
Sezione di Farmaceutica e Nutraceutica
Via U. Schiff, 6 - 50019 Sesto F.no - Firenze
Type of Assessment - Last names A-L
The verification of acquired skills and knowledge consists of an oral examination that takes into account the laboratory tests (with related reports).
Type of Assessment - Last names M-Z
The verification of acquired skills and knowledge consists of an oral examination that takes into account the laboratory tests (with related reports).
Course program - Last names A-L
Safety regulations and first aid rules in chemical laboratory.
“Monograph” in European Pharmacopoiea and in Farmacopea Ufficiale Italiana
Preliminary tests: organoleptic examination, behavior to the heating, organic elemental analysis (Lassaigne test), metal analysis, physical properties determination, dissolution tests.
Salts analysis (organic and metallorganic compounds).
Chemical Analysis for the characterization of olefin and phenyl groups, hydroxyl function (alcohol, phenol), carbonyl function (aldehyde, ketone), carboxyl function (carboxyl acid and functional derivatives), aminic function (primary, secondary, tertiary, aliphatic and aromatic amines), sulfonamides, nitroderivatives.
Analysis of pharmaceutical structures and of some drug classes FUI and EP: Acetates, Alkaloids, Amino Acids, Barbiturates, Benzoates, Carbohydrates, Citrates, Lactates, Phenols, Polyalcohol derivatives, Pyrazolone derivatives, Pyridine and Pyrimidine derivatives, Salicylates, Sulfonamides, Tartrates, Xanthine.
Basic knowledge and applications of instrumental technologies for the characterization of pharmaceuticals: IR spectroscopy. An outline of the 1H-NMR and MS.
Explanation of the Tables, utilized in laboratory, for identification of unknown compounds.
Systematic procedure to identification of pharmaceuticals registered in the European Pharmacopoeia VII.
“Monograph” in European Pharmacopoiea and in Farmacopea Ufficiale Italiana
Preliminary tests: organoleptic examination, behavior to the heating, organic elemental analysis (Lassaigne test), metal analysis, physical properties determination, dissolution tests.
Salts analysis (organic and metallorganic compounds).
Chemical Analysis for the characterization of olefin and phenyl groups, hydroxyl function (alcohol, phenol), carbonyl function (aldehyde, ketone), carboxyl function (carboxyl acid and functional derivatives), aminic function (primary, secondary, tertiary, aliphatic and aromatic amines), sulfonamides, nitroderivatives.
Analysis of pharmaceutical structures and of some drug classes FUI and EP: Acetates, Alkaloids, Amino Acids, Barbiturates, Benzoates, Carbohydrates, Citrates, Lactates, Phenols, Polyalcohol derivatives, Pyrazolone derivatives, Pyridine and Pyrimidine derivatives, Salicylates, Sulfonamides, Tartrates, Xanthine.
Basic knowledge and applications of instrumental technologies for the characterization of pharmaceuticals: IR spectroscopy. An outline of the 1H-NMR and MS.
Explanation of the Tables, utilized in laboratory, for identification of unknown compounds.
Systematic procedure to identification of pharmaceuticals registered in the European Pharmacopoeia VII.
Course program - Last names M-Z
Safety regulations and first aid rules in chemical laboratory.
“Monograph” in European Pharmacopoiea and in Farmacopea Ufficiale Italiana
Preliminary tests: organoleptic examination, behavior to the heating, organic elemental analysis (Lassaigne test), metal analysis, physical properties determination, dissolution tests.
Salts analysis (organic and metallorganic compounds).
Chemical Analysis for the characterization of olefin and phenyl groups, hydroxyl function (alcohol, phenol), carbonyl function (aldehyde, ketone), carboxyl function (carboxyl acid and functional derivatives), aminic function (primary, secondary, tertiary, aliphatic and aromatic amines), sulfonamides, nitroderivatives.
Analysis of pharmaceutical structures and of some drug classes FUI and EP: Acetates, Alkaloids, Amino Acids, Barbiturates, Benzoates, Carbohydrates, Citrates, Lactates, Phenols, Polyalcohol derivatives, Pyrazolone derivatives, Pyridine and Pyrimidine derivatives, Salicylates, Sulfonamides, Tartrates, Xanthine.
Basic knowledge and applications of instrumental technologies for the characterization of pharmaceuticals: IR spectroscopy. An outline of the 1H-NMR and MS.
Explanation of the Tables, utilized in laboratory, for identification of unknown compounds.
Systematic procedure to identification of pharmaceuticals registered in the European Pharmacopoeia VII.
“Monograph” in European Pharmacopoiea and in Farmacopea Ufficiale Italiana
Preliminary tests: organoleptic examination, behavior to the heating, organic elemental analysis (Lassaigne test), metal analysis, physical properties determination, dissolution tests.
Salts analysis (organic and metallorganic compounds).
Chemical Analysis for the characterization of olefin and phenyl groups, hydroxyl function (alcohol, phenol), carbonyl function (aldehyde, ketone), carboxyl function (carboxyl acid and functional derivatives), aminic function (primary, secondary, tertiary, aliphatic and aromatic amines), sulfonamides, nitroderivatives.
Analysis of pharmaceutical structures and of some drug classes FUI and EP: Acetates, Alkaloids, Amino Acids, Barbiturates, Benzoates, Carbohydrates, Citrates, Lactates, Phenols, Polyalcohol derivatives, Pyrazolone derivatives, Pyridine and Pyrimidine derivatives, Salicylates, Sulfonamides, Tartrates, Xanthine.
Basic knowledge and applications of instrumental technologies for the characterization of pharmaceuticals: IR spectroscopy. An outline of the 1H-NMR and MS.
Explanation of the Tables, utilized in laboratory, for identification of unknown compounds.
Systematic procedure to identification of pharmaceuticals registered in the European Pharmacopoeia VII.